土壤中有机氯农药残留的分析技术研究进展

百花草

[align=justify]摘　要：文章总结了近年来土壤中有机氯农药残留分析的样品前处理和测定方法的研究进展,重点阐述微波萃取法、加速溶剂萃取法、固相萃取法、固相微萃取法、基质固相分散萃取法、超临界流体萃取法等前处理技术及气相色谱技术、气相色谱-质谱联用技术等在土壤中有机氯农药残留分析中的应用,指出了未来的发展趋势.
关键词：有机氯农药残留;土壤;样品前处理方法;分析技术
分类号：O656.31;X131.3 　文献标识码：A
文章编号：0254-5357(2009)02-0151-06

Progresses on Organochlorine Pesticide Residue Analysis for Soil Samples

CHEN Wei-ming　 DENG Tian-long　 ZHANG Qin　 LI Qing-xia　

基金项目：国家自然科学基金项目资助(40573044);四川省应用基础研究基金项目资助(05JY029-089-1);中央级公益性科研院所基本科研业务费专项资金资助(AS2007J5) 作者简介：陈卫明(1982-),女,吉林梅河口人,在读硕士研究生,分析化学专业.E-mail:chenweiming320@163.com. 作者简介：邓天龙(1966-),男,四川仪陇人,教授,博士生导师,主要从事矿产资源综合利用和环境污染化学研究.E-mail:tldeng@isl.ac.cn.通讯作者. 作者单位：陈卫明（成都理工大学材料与化学化工学院,四川,成都,610059;中国地质科学院地球物理地球化学勘查研究所,河北,廊坊,065000）　 　　　　　邓天龙（成都理工大学材料与化学化工学院,四川,成都,610059;中国科学院青海盐湖研究所,青海,西宁,810008）　 　　　　　张勤（中国地质科学院地球物理地球化学勘查研究所,河北,廊坊,065000）　 　　　　　李庆霞（中国地质科学院地球物理地球化学勘查研究所,河北,廊坊,065000）　 参考文献： [align=justify][1]吴德生.内分泌干扰物与人类健康[J].环境与健康杂志,2001,18(4):201-203. [2]吴春先,慕立义.我国农药残留分析技术发展概述[J].农药科学与管理,2002,23(2):13-16. [3]Ganzler K,Sago A,Valko K.Microwave extraction:A novel sample preparation method for chromatography[J].Journal of Chromatography,1986,371(1):299-306. [4]孙萍,肖波,杨家宽.化工环保[M].北京:化学工业出版社.2002. [5]Lopez-Avila V,Young R,Beckert W F.Stability of organic pollutants during microwave-assisted extraction from sojld matrices[J].Jounrnal of AOAC International,1998,81(2):462-476. 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